Contributors .................................................. vii
Preface ........................................................ ix
1 Recent Developments in Liquid-State INADEQUATE Studies ....... 1
Dušan Uhrín
1 Introduction .............................................. 2
2 INADEQUATE-The Basic Concept .............................. 3
3 Increasing the Sensitivity of INADEQUATE .................. 4
4 Measurement of 13C-13C Coupling Constants ................. 14
5 Applications of High-Resolution INADEQUATE to 13C ........ 19
6 Applications of INADEQUATE to Nuclei Other Than 13C ...... 26
7 Outlook .................................................. 32
References .................................................. 32
2 Phosphorus-31 NMR Spectroscopy of Condensed Matter .......... 35
Marek J. Potrzebowski, Sławomir Kaźmierski, Hassan
Kassassir, and Beata Miksa
1 Introduction ............................................. 36
2 Progress in Methodology .................................. 37
3 Applications of 13P SS NMR Spectroscopy .................. 55
4 Concluding Remarks ...................................... 107
Acknowledgement ............................................ 107
References ................................................. 107
3 Recent Applications of Solid-State 170 NMR ................. 115
K. Yamada
1 Introduction ............................................ 116
2 17O Synthesis ........................................... 118
3 Background of Solid-State 17O NMR ....................... 120
4 Fundamentals of 17O NMR in Biological Solids ............ 127
5 Applications of Solid-State 17O NMR in Biochemistry ..... 148
6 Conclusions ............................................. 155
References ................................................. 156
4 Spatial Inhomogeneity of Cavities in Polymer Network
Systems as Characterised by Field-Gradient NMR Using
Probe Diffusant Molecules and Polymers with Different
Sizes ...................................................... 159
Kazuhiro Kamiguchi, Shigeki Kuroki, Yuji Yamane, Mitsuru
Satoh, and Isao Ando
1 Intro'duction ........................................... 160
2 Network Structure of Polymer Gels and Diffusional
Behaviour of Probe Polymers ............................. 161
3 Network Structure of Micrometre-Scale Cavity Obtained
from Phase-Separated Polymer Blends as Characterised
by Using Probe Molecules ................................ 192
4 Conclusions ............................................. 199
References ................................................. 199
5 Practical NMR Analysis of Morphology and Structure of
Polymers ................................................... 203
Takeshi Yamanobe, Hiroki Uehara, and Masaki Kakiage
1 Introduction ............................................ 204
2 Analysis Method of Free Induction Decay of Pulse NMR
for Polymers ............................................ 206
3 Morphology and Relaxation Behaviour ..................... 210
4 Kinetics of Dynamic Process of Polymers ................. 229
5 Conclusions ............................................. 238
References ................................................. 238
Subject Index ................................................. 241
|
