Nitsche F. Synthetic and crystal chemical approach towards iron selenide and iron arsenide compounds with Anti-PbO-Type motifs: Diss. Dr. rer. nat. - Dresden: Techn. Univ., 2012. - viii, 122 p.: ill., graph. - Ref.: p.113-122.  Место хранения:   024 | Институт неорганической химии им. А.В.Николаева CO РАН | Новосибирск

Оглавление / Contents

1 Introduction and Motivation .................................. 1 2 Room-Temperature Synthesis and Properties of Metastable FeSe ........................................................ 15 2.1 Introduction ........................................... 15 2.2 Experimental ........................................... 16 2.3 Results and Discussion ................................. 20 2.4 Conclusion ............................................. 31 3 Structural Trends of REFeAsO ................................ 33 3.1 Introduction ........................................... 33 3.2 Experimental ........................................... 35 3.3 Results ................................................ 37 3.4 Discussion ............................................. 42 3.5 Conclusion ............................................. 49 4 Tetragonal to Orthorhombic Transition of GdFeAsO ............ 51 4.1 Introduction ........................................... 51 4.2 Experimental ........................................... 53 4.3 Results and Discussion ................................. 53 4.4 Conclusion ............................................. 61 5 Transport Anisotropy of Large LaFeAsO Single Crystals ....... 63 5.1 Introduction ........................................... 63 5.2 Experimental ........................................... 63 5.3 Results and Discussion ................................. 64 5.4 Conclusion ............................................. 67 6 Summary and Outlook ......................................... 69 7 Acknowledgement ............................................. 71 8 List of Publications ........................................ 73 Appendices ..................................................... 75 A Treatment of Synchrotron Data ............................ 77 B Reconstruction of Reciprocal Space ....................... 81 C Evaluation of Reflection Splitting ....................... 85 D Additional X-Ray Diffraction Data ........................ 89 D.l Rietveld Refinement of FeSe ......................... 89 D.2 Single-Crystal X-ray Diffraction Data of REFeAsO .... 92 D.3 Synchrotron Data of GdFeAsO at Different Temperatures ....................................... 100 References .................................................... 113